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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 991601Generated: October 31, 2026

HCID 22036340, compound → HCID 131723546, compound

https://huagongshe.com/reaction/991601

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22036340HCID 22036340—
SolventWaterHCID 962—
ProductHCID 131723546HCID 131723546—

Reaction Steps

The title compound was prepared according to the procedure described in Example 1, Step 2, starting from 2-chloro-3-(2-phenoxyethoxy)quinoxaline (0.65 g, 2.15 mmol): yield 0.44 g (58%) as the free base. A portion of the free base was converted to its hydrochloride salt: mp 123-126° C.; HRMS m/z calcd for C20H22N4O2 (M)+ 350.1743, found 350.1748. Anal. (C20H22N4O2 1.75 HCl. 0.5 H2O) C, H, N.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06465467B1
Source datasetuspto-grants-2002_10
ORD IDord-e124e205dfee4233a086b467048cb21f
Source noteuspto-grants-2002_10