HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22036340, compound → HCID 131723546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22036340 | HCID 22036340 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131723546 | HCID 131723546 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1, Step 2, starting from 2-chloro-3-(2-phenoxyethoxy)quinoxaline (0.65 g, 2.15 mmol): yield 0.44 g (58%) as the free base. A portion of the free base was converted to its hydrochloride salt: mp 123-126° C.; HRMS m/z calcd for C20H22N4O2 (M)+ 350.1743, found 350.1748. Anal. (C20H22N4O2 1.75 HCl. 0.5 H2O) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465467B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-e124e205dfee4233a086b467048cb21f |
| Source note | uspto-grants-2002_10 |