Ethylene carbonate → HCID 233168, compound

HRID 991644Notes

Reaction equation

[CH2:1]1[O:5][C:4]2[CH:6]=[C:7]([OH:10])[CH:8]=[CH:9][C:3]=2[O:2]1.C1(=O)O[CH2:14][CH2:13][O:12]1>>[O:2]1[C:3]2[CH:9]=[CH:8][C:7]([O:10][CH2:14][CH2:13][OH:12])=[CH:6][C:4]=2[O:5][CH2:1]1

Participants

Reactant 2

HCID 7303Ethylene carbonate

HCID 68289Sesamol

Product 1

HCID 233168HCID 233168, compoundYield 99%

Procedure

The title compound was prepared according to the procedure of Example 114, Step 1 starting from sesamol (2.0 g, 14.5 mmol ) and ethylene carbonate (1.0 g, 11.4 mmol): solid; yield 99%. MS m/z 182 (M)+.

Sources & evidence

ORD record: ord-59169841cd4e4e6abdab7b9e2fe40e0d
Source dataset: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06465467B1

Reaction notes

Loading…