HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenoxyethanol → HCID 131723553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenoxyethanol | HCID 31236 | — |
| Reactant | HCID 87650681 | HCID 87650681 | — |
| Product | HCID 131723553 | HCID 131723553 | 68% |
Reaction Steps
The title compound was prepared starting from 2-phenoxy-1-ethanol and 3-chloro-2-[4-tert-butoxycarbonyl-(2S)-methyl-1-piperazinyl]pyrazine (prepared according to the procedure of Example 172, Step 2, with the exception that (2S)-methylpiperazine was substituted for (2R)-methylpiperazine). MS m/z 315 (M+H)+. Yield 68%; mp 162-163° C. Anal. (C17H22N4O2.HCl) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465467B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-06be1a9416044541b5ec6425608e29c1 |
| Source note | uspto-grants-2002_10 |