HRID991758

反应详情

EQUATION

反应方程式

HRID 991758 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The title material from Step A was dissolved in methanol with catalytic amount of 10% Pd on C. The reaction mixture was hydrogenated for 2 hours at room temperature in methanol under 25 psi of hydrogen. After filtration of the crude reaction mixture through a pad of Celite, the solvent was evaporated under reduced pressure to afford the title compound.

WORKUP

后处理

  1. filtrationAfter filtration of the crude
  2. customreaction mixture through a pad of Celite
  3. customthe solvent was evaporated under reduced pressure