HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Tyrosine 1,1-dimethylethyl ester → HCID 57013426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Tyrosine 1,1-dimethylethyl ester | HCID 6950582 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57013426 | HCID 57013426 | — |
Reaction Steps
L-Tyrosine tert-butyl ester (0.6 g) was hydrogenated in MeOH, with 10% Rh/Al2O3 under 50 psi of hydrogen at room temperature for 2 days. The reaction mixture was filtered through Celite and the solvent evaporated under reduced pressure to afford the title intermediate as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465513B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-eef00932c1b0431ab82cbd42b4c8ba7f |
| Source note | uspto-grants-2002_10 |