HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoroboric acid → HCID 178444241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoroboric acid | HCID 28118 | — |
| Reactant | 2-Bromo-6-fluoronaphthalene | HCID 345397 | — |
| Reactant | 4-Pentylcyclohexanone | HCID 566097 | — |
| Reactant | 5,6-Difluoro-2-bromonaphthalene | HCID 11413832 | — |
| Reactant | 6-Bromo-1-fluoro-2-naphthylamine | HCID 54558670 | — |
| Product | HCID 178444241 | HCID 178444241 | — |
Reaction Steps
The procedure of Example 14 was followed except that 5,6-difluoro-2-bromonaphthalene (synthesized by converting 6-bromo-1-fluoro-2-naphthylamine to a diazonium salt of tetrafluoroboric acid, and then subjecting the diazonium salt to thermal decomposition) was used instead of 6-fluoro-2-bromonaphthalene and 4-pentylcyclohexanone was used instead of 4-propylcyclohexanone to obtain 5,6-difluoro-2-(trans-4-pentylcyclohexyl)naphthalene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06468607B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-5fbe548ca2934496a942363082bbe259 |
| Source note | uspto-grants-2002_10 |