HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54131529, compound → HCID 18411541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54131529 | HCID 54131529 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18411541 | HCID 18411541 | — |
Reaction Steps
A mixture of [2,4′]bithiazol-2′-ylmethanol (1.53 g; 7.72 mmol), obtained as described in the above step, and MnO2 (13.93 g; 160.2 mmol) in CH2Cl2 (76.5 ml) and methanol (7.65 ml) was stirred at room temperature for about 23 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06468979B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-eb742919384d4db18d602df05edb5984 |
| Source note | uspto-grants-2002_10 |