Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 86759978 | HCID 86759978 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 69628011 | HCID 69628011 | — |
Reaction Steps
A solution comprised of methyl 7-fluoro-6-(2-methyl-phenylamino)-benzo[1,2,5]oxadiazole-5-carboxylate 2-oxide and sodium azide (1.38 equiv.) in ethylene glycol is heated to 140-150° C. for 30 minutes to obtain, after column chromatography, the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06469004B1 |
|---|
| Source dataset | uspto-grants-2002_10 |
|---|
| ORD ID | ord-5fd0ee10bafd49809bbe3c24295264de |
|---|
| Source note | uspto-grants-2002_10 |
|---|
