Methylamine → HCID 11450215, compound

HRID 992765Notes

Reaction equation

[CH3:1][O:2]/[N:3]=[C:4](\[C:9]1[C:14]([CH3:15])=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:16][O:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[CH3:24])/[C:5](OC)=[O:6].[CH3:25][NH2:26]>>[CH3:1][O:2]/[N:3]=[C:4](\[C:9]1[C:14]([CH3:15])=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:16][O:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[CH3:24])/[C:5]([NH:26][CH3:25])=[O:6]

Participants

Reactant 2

HCID 6329Methylamine

HCID 11198199HCID 11198199, compound

Product 1

HCID 11450215HCID 11450215, compound

Procedure

methyl E-2-((2-methylphenyl)oxymethyl)-6-methylphenylglyoxylate O-methyl oxime prepared in the step 1 is reacted with methylamine (NH2Me) to give N-methyl E-2-((2-methylphenyl)oxymethyl)-6-methylphenylglyoxylamide O-methyl oxime of the present invention (step 2).

Sources & evidence

ORD record: ord-57ef3d25ef73450f94b35494a2940ae2
Source dataset: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06469209B1

Reaction notes

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