HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178443619, compound → Phenetole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178443619 | HCID 178443619 | — |
| Solvent | Hexamethylphosphorous triamide | HCID 15355 | — |
| Product | Phenetole | HCID 7674 | 86% |
Reaction Steps
The reaction was carried out completely in the same manner as in Example 1, except that tris[tris(dimethylamino)phosphoranylideneamino](dioctylamino)phosphoranylideneamino phosphonium ethoxide: [(Me2N)3P═N]3P+{N═P[N(C8H17)2]}, C2H5O− was used instead of tetrakis[tris(dimethylamino)phosphoranylideneamino]phosphonium methoxide in Example 1. Objective ethoxybenzene was produced in the yield of 86%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06469224B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-673f3a6c71334a6790f2aa54d40eeb68 |
| Source note | uspto-grants-2002_10 |