HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Trifluoromethylphenyl)-3-buten-2-one → 4-[2-(Trifluoromethyl)phenyl]butan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Trifluoromethylphenyl)-3-buten-2-one | HCID 522612 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-[2-(Trifluoromethyl)phenyl]butan-2-one | HCID 11746021 | — |
Reaction Steps
200 mg of Raney nickel are added to a solution of 2.05 g of 4-(2-trifluoromethylphenyl)-3-buten-2-one in 100 ml of ethyl acetate and the mixture is stirred under a hydrogen atmosphere and at standard pressure for 7 h. The mixture is subsequently filtered and the filtrate is evaporated under reduced pressure, whereby the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091371B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-456684d1f9d94974b8fd4c859ea625b7 |
| Source note | uspto-grants-2006_08 |