HRID9928

反应详情

EQUATION

反应方程式

HRID 9928 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

200 mg of Raney nickel are added to a solution of 2.05 g of 4-(2-trifluoromethylphenyl)-3-buten-2-one in 100 ml of ethyl acetate and the mixture is stirred under a hydrogen atmosphere and at standard pressure for 7 h. The mixture is subsequently filtered and the filtrate is evaporated under reduced pressure, whereby the title compound is obtained.

WORKUP

后处理

  1. filtrationThe mixture is subsequently filtered
  2. customthe filtrate is evaporated under reduced pressure, whereby the title compound
  3. customis obtained