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HRID992982

反应详情

EQUATION

反应方程式

HRID 992982 的结构方程式

REACTANTS

反应物

3
结构：O=C(OOC(=O)c1ccccc1)c1ccccc1
HCID7187

Benzoyl peroxide

C14H10O4

结构：O=C1CCC(=O)N1Br
HCID67184

1-Bromopyrrolidine-2,5-dione

C4H4BrNO2

结构：Cc1ccc2ncoc2c1
HCID2724969

6-Methylbenzoxazole

C8H7NO

PRODUCTS

生成物

1
结构：BrCc1ccc2ncoc2c1
HCID21985057

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)(Cl)Cl
溶剂HCID5943

Carbon tetrachloride

CCl4

PROCEDURE

实验过程

6-Methylbenzoxazole was reacted with NBS (1 eq) and catalytic amount of benzoyl peroxide in CCl4 at 90° C. for 12 h to obtain 6-bromomethylbenzoxazole which was purified by flash chromatography (EtOAc:Hexane=1:5).