HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 2-(2-Chloro-6-methoxyphenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-Chloro-6-methoxybenzeneacetonitrile | HCID 22327511 | — |
| Product | 2-(2-Chloro-6-methoxyphenyl)acetic acid | HCID 22327488 | — |
Reaction Steps
325 g of 2-chloro-6-methoxyphenylacetonitrile are reacted with 171 g of potassium hydroxide in 690 ml of ethylene glycol. 331 g of solid are obtained (m.p. 164-165° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06472419B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-e0f184c48bd34a22ab4d74065af3a5f3 |
| Source note | uspto-grants-2002_10 |