HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 2-(2-Chloro-4-methoxyphenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | (2-Chloro-4-methoxyphenyl)acetonitrile | HCID 22327506 | — |
| Product | 2-(2-Chloro-4-methoxyphenyl)acetic acid | HCID 4209132 | — |
Reaction Steps
657 g (purity 75%) of 2-chloro-4-methoxyphenylacetonitrile are reacted with 303 g of potassium hydroxide in 1308 ml of ethylene glycol. 430 g of solid are obtained (m.p.: 83-86° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06472419B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-e461ea3cd6c24fc3b0ca8ea67d8fff7c |
| Source note | uspto-grants-2002_10 |