HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70128057, compound → HCID 10181214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70128057 | HCID 70128057 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 10181214 | HCID 10181214 | — |
Reaction Steps
A solution of the ester 1-9(110 mg) in dichloromethane (10 mL) and trifluoroacetic acid (10 mL) were stirred at room temperature for 2 hours. The mixture was concentrated in vacuo, dissolved in water, frozen and lyophilized to give 1-10as a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06472403B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-2b9be4888e434efdbe7db290cbbbbe29 |
| Source note | uspto-grants-2002_10 |