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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 993469Generated: October 29, 2026

HCID 18409266, compound → HCID 18409316, compound

https://huagongshe.com/reaction/993469

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18409266HCID 18409266—
CatalystPalladiumHCID 23938—
ProductHCID 18409316HCID 1840931690%

Reaction Steps

An ethanol solution of Example 195 compound (260 mg, 0.49 mmol) containing 50 mg of 10% palladium on carbon was stirred under a hydrogen atmosphere (balloon) for 14 hrs. The reaction was filtered through a 0.2 μm nylon filter to remove the catalyst and the solvent evaporated yielding 235 mg (90%) of title compound as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06472414B1
Source datasetuspto-grants-2002_10
ORD IDord-647aa2b45d8648398e0092b1cd8ba9d2
Source noteuspto-grants-2002_10