HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18409266, compound → HCID 18409316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18409266 | HCID 18409266 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18409316 | HCID 18409316 | 90% |
Reaction Steps
An ethanol solution of Example 195 compound (260 mg, 0.49 mmol) containing 50 mg of 10% palladium on carbon was stirred under a hydrogen atmosphere (balloon) for 14 hrs. The reaction was filtered through a 0.2 μm nylon filter to remove the catalyst and the solvent evaporated yielding 235 mg (90%) of title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06472414B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-647aa2b45d8648398e0092b1cd8ba9d2 |
| Source note | uspto-grants-2002_10 |