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HRID994

反应详情

EQUATION

反应方程式

HRID 994 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccc([N+](=O)[O-])cc1S(=O)(=O)O
HCID8458

2-Methyl-5-nitrobenzenesulfonic acid

C7H7NO5S

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：[K+].[O]=[Mn](=[O])(=[O])[O-]
HCID516875

Potassium permanganate

KMnO4

PRODUCTS

生成物

1
结构：O=C(O)c1c([N+](=O)[O-])cccc1S(=O)(=O)O
HCID19693800

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

400.0 g (2.53 mol) of potassium permanganate are added in portions at 80° C. over a period of 2 h to a solution of 106.0 g (0.40 mol) of 2-methyl-5-nitrobenzenesulfonic acid and 80.0 g (0.58 mol) of potassium carbonate in 1300 ml of water. The reaction temperature is maintained at between 80° and 95° C.

WORKUP

后处理

  1. temperatureThe reaction temperature is maintained at between 80° and 95° C.