钙 → HCID 70503069，化合物
反应方程式
[Ca:1].[CH3:2][C:3]1[S:10][C:9]2[S:8](=[O:12])(=[O:11])[NH:7][C:6](=[O:13])[C:5]=2[CH:4]=1>CO>[Ca:1].[CH3:2][C:3]1[S:10][C:9]2[S:8](=[O:12])(=[O:11])[NH:7][C:6](=[O:13])[C:5]=2[CH:4]=1参与物
4
实验过程
500 ml of methanol were added to 0.49 gm (12.3 millimols) of calcium, the mixture was refluxed, and 5.0 gm (24.6 millimols) of 5-methyl-thieno[3,2-d]isothiazole-3(2H)-one-1,1-dioxide were added to the suspension thus obtained. The resulting solution was evaporated, and the residue was recrystallized from a little ethanol/ether. 3.9 gm (71% of theory) of 5-methyl-thieno[3,2-d]-isothiazole-3(2H)-one-1,1-dioxide calcium salt were obtained.
后处理
- temperaturethe mixture was refluxed
- customthus obtained
- customThe resulting solution was evaporated
- customthe residue was recrystallized from a little ethanol/ether
来源与证据
- ORD记录
- ord-ba3505421a60488e94663e95d1061360
- 来源数据集
- uspto-grants-1984_02
- 专利号
- US04430355
反应笔记
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