N-羟基邻苯二甲酰亚胺 → O-[(1,3-Thiazol-4-yl)methyl]hydroxylamine--hydrogen chloride (1/1)

HRID 1663114笔记

反应方程式

HRID 1663114 反应方程式
[OH:1][N:2]1C(=O)C2=CC=CC=C2C1=O.Cl.[Cl:14][CH2:15][C:16]1[N:17]=[CH:18][S:19][CH:20]=1>>[ClH:14].[S:19]1[CH:20]=[C:16]([CH2:15][O:1][NH2:2])[N:17]=[CH:18]1

参与物

3

反应物 2

HCID 10665N-羟基邻苯二甲酰亚胺HCID 27632894-氯甲基噻唑盐酸盐

产物 1

HCID 54604191O-[(1,3-Thiazol-4-yl)methyl]hydroxylamine--hydrogen chloride (1/1)

实验过程

Prepared by a similar procedure as described for preparation 18. Starting materials: N-hydroxyphthalimide and 4-(chloromethyl)thiazole hydrochloride (TCl). 13C-NMR (DMSO-d6) δ 155.1, 149.2, 121.4, 70.3.

后处理

  1. customPrepared by a similar procedure
  2. customas described for preparation 18

来源与证据

ORD记录
ord-58b55d0b54fb4618998d0116035e8ca7
来源数据集
uspto-grants-2011_10
专利号
US08034811B2

反应笔记

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