氢氧化钾 → 2-Pyridinecarboxylic acid, potassium salt (1:1)

HRID 398317笔记

反应方程式

HRID 398317 反应方程式
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3](C([O-])=O)[C:2]=1[C:10]([O-:12])=[O:11].[OH-].[K+:14]>CO>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:10]([O-:12])=[O:11].[K+:14]

参与物

4

反应物 2

HCID 14797氢氧化钾HCID 5460301HCID 5460301，化合物

产物 1

HCID 236723372-Pyridinecarboxylic acid, potassium salt (1:1)

试剂、催化剂与溶剂 1

HCID 887Methanol溶剂

实验过程

The pyridinedicarboxylate 30 (19.5 g, 0.1 mol) was treated with solid KOH (6.51 g, 0.1 mol) in 300 mL of methanol at room temperature for 2 h, giving rise to a thick pale white suspension, which was filtered and dried to provide the mono-potassium pyridinecarboxylate 3 in quantitative yield.

后处理

  1. customgiving rise to a thick pale white suspension, which
  2. filtrationwas filtered
  3. customdried

来源与证据

ORD记录
ord-b6da16e1fb1843f5a34cc89c2543b55a
来源数据集
uspto-grants-2003_08
专利号
US06610883B1

反应笔记

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