2,4-二氯-6-硝基苯胺 → 10,12-Dichlorodibenzo[a,c]phenazine
反应方程式
[Cl:1][C:2]1[CH:8]=[C:7]([Cl:9])[CH:6]=[C:5]([N+:10]([O-])=O)[C:3]=1[NH2:4].[C:13]1(=O)[C:26]2[CH:25]=[CH:24][C:23]3[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=3)[C:17]=2[CH:16]=[CH:15][C:14]1=O>CC(C)=O>[Cl:1][C:2]1[CH:8]=[C:7]([Cl:9])[CH:6]=[C:5]2[C:3]=1[N:4]=[C:24]1[C:25](=[N:10]2)[C:26]2[CH:13]=[CH:14][CH:15]=[CH:16][C:17]=2[C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][C:23]1=2参与物
4
实验过程
When 0.12 mole each of 2,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 24 g. (81 percent yield) of 10,12-dichlorodibenzo[a,c]phenazine, mp = 221°-222° C. (acetone), were obtained.
来源与证据
- ORD记录
- ord-cf5c608cf4994a89b522be502c1d94b8
- 来源数据集
- uspto-grants-1977_12
- 专利号
- US04064127
反应笔记
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