2,6-二甲氧基苯甲醛 → HCID 69082306，化合物

HRID 594635

反应方程式

HRID 594635 反应方程式
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][NH2:12].[CH3:13][O:14][C:15]1[CH:22]=[CH:21][CH:20]=[C:19]([O:23][CH3:24])[C:16]=1[CH:17]=O>>[CH3:13][O:14][C:15]1[CH:22]=[CH:21][CH:20]=[C:19]([O:23][CH3:24])[C:16]=1[CH:17]1[N:12]([CH2:11][C:2]2[CH:3]=[CH:4][C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[CH:1]=2)[C:15](=[O:14])[CH2:16][CH2:19][CH2:20]1

参与物

3

反应物 2

HCID 964042,6-二甲氧基苯甲醛HCID 1372821-(2-萘基)甲胺

产物 1

HCID 69082306HCID 69082306，化合物

实验过程

Prepared according to the described general procedure 6 (GP6) with commercially available naphthalen-2-ylmethanamine and commercially available 2,6-dimethoxybenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions H): tR=1.35 min.; [M+H]+: 375.79 g/mol.

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound

来源与证据

ORD记录
ord-0d1651c645b5490f981780cc2d70909e
来源数据集
uspto-grants-2016_01
专利号
US09242970B2

关联笔记

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