Reaktionsgleichung
[OH-].[Na+].C(OCCCCCCCCCCCC)(=O)C1C=C(O)C(O)=[C:6]([OH:7])C=1.C(OC(C1C=CC=CC=1)C(=O)C1C=CC=CC=1)C.[N:45]1[C:52]([NH2:53])=[N:51][C:49]([NH2:50])=[N:48][C:46]=1[NH2:47].C=O>O>[CH2:6]=[O:7].[N:45]1[C:52]([NH2:53])=[N:51][C:49]([NH2:50])=[N:48][C:46]=1[NH2:47]Komponenten
Edukt 5
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 60 °C
Versuchsvorschrift
To 100 parts of an aqueous solution of pH 4.0 containing 5% of a styrene-maleic anhydride copolymer and a small amount of sodium hydroxide was added a mixed solution consisting of 10 parts of dodecyl gallate, 30 parts of a polyoxypropylene glycol monoether, 0.3 part of benzoin ethyl ether and 59.7 parts of an epoxy acrylate type photocurable resin (brand name: RIPOXY, manufactured by Showa Highpolymer Co., Ltd.), and they were emulsified. 10 parts of melamine, 25 parts of a 37% aqueous formaldehyde solution and 65 parts of water were adjusted to pH 9 with sodium hydroxide and then heated to 60° C. In 15 minutes, the mixture became transparent and a melamine-formaldehyde precondensate was obtained. This precondensate was added to the emulsion prepared previously. The resulting mixture was continuously stirred at 60° C. The formation of microcapsules was confirmed in 30 minutes and the microcapsule fluid was cooled to room temperature.
Quellen und Nachweise
- ORD-Eintrag
- ord-6805994fe59045298bc36e284a3c45c7
- Quelldatensatz
- uspto-grants-1990_10
- Patentnummer
- US04963457
Verknüpfte Notizen
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