1-Dodecanethiol → Dibutyltin bis(lauryl mercaptide)
Reaktionsgleichung
[CH2:1]([Sn:5](=O)[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].[CH2:11]([SH:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>O>[CH2:1]([Sn:5]([CH2:6][CH2:7][CH2:8][CH3:9])([S:23][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[S:23][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:2][CH2:3][CH3:4]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
This compound was prepared from di-n-butyltin-oxide and 1 dodecanethiol by azeotropic removal of water using the method described in U.S. Pat. No. 2,648,650. All spectroscopic and analytical data were consistent with the proposed structure.
Quellen und Nachweise
- ORD-Eintrag