Iodobenzene → N-(2-(Dimethylamino)ethyl)aniline

Temperatur

100 °C

In a 50 mL round-bottomed flask (t=g) was unsym-Dimethylethylenediamine (1.080 mL, 9.80 mmol), Iodobenzene (0.549 mL, 4.90 mmol), and TRIS(DIBENZYLIDENEACETONE)DIPALLADIUM(0) (0.449 g, 0.49 mmol)Cesium carbonate (2.396 g, 7.35 mmol) andCesium carbonate (2.396 g, 7.35 mmol) were added. in DMF (10 mL) ([VOLUME]) to give a brown suspension. Reaction stirred over night at 100°C. no reaction.

ORD-Eintrag

ord-6eea29be7d4b47c5893b1e243ef41836

Quelldatensatz

750 AstraZeneca ELN dataset

Originallink

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