Water → 4-(Hexyloxy)benzohydrazide

HRID 1386610Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1386610
[CH2:1]([O:7][C:8]1[CH:17]=[CH:16][C:11]([C:12](OC)=[O:13])=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].O.[NH2:19][NH2:20].O>C(O)C>[CH2:1]([O:7][C:8]1[CH:17]=[CH:16][C:11]([C:12]([NH:19][NH2:20])=[O:13])=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Komponenten

5

Edukt 3

HCID 962WaterHCID 24654Hydrazine hydrate (1:1)HCID 3576592Methyl 4-hexyloxybenzoate

Produkt 1

HCID 16259404-(Hexyloxy)benzohydrazideAusbeute 98 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

A solution of Methyl 4-n-hexyloxybenzoate (2.00 g) and hydrazine hydrate (4.24 g) in ethanol (10 ml) was refluxed for 6 hours. After cooling, the reaction mixture was poured into water. The precipitate was collected by filtration, washed with water and dried over P2O5 under reduced pressure to give N-(4-n-hexyloxybenzoyl)hydrazine (1.96 g).

Aufarbeitung

  1. temperatureAfter cooling
  2. filtrationThe precipitate was collected by filtration
  3. washwashed with water
  4. dry with materialdried over P2O5 under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-081ca8b4dd844ba1951693d1764ab00c
Quelldatensatz
uspto-grants-2001_07
Patentnummer
US06265536B1

Notizen zur Reaktion

Wird geladen…