Sulfuric Acid → Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride

HRID 1418629

Reaktionsgleichung

Reaktionsgleichung von HRID 1418629
COC(C1SC=CC=1S(NCC1C=CC2OCOC=2C=1)(=O)=O)=O.S(=O)(=O)(O)O.[C:29]([NH2:33])(=[O:32])[CH:30]=[CH2:31].[Cl-:34].[C:35]([O:39][CH2:40][CH2:41][N+:42]([CH3:45])([CH3:44])[CH3:43])(=[O:38])[CH:36]=[CH2:37].Br([O-])(=O)=O.[Na+].[Na+].[Na+].[Na+].[Na+].C(N(CC([O-])=O)CC([O-])=O)CN(CC([O-])=O)CC([O-])=O>O>[Cl-:34].[C:35]([O:39][CH2:40][CH2:41][N+:42]([CH3:44])([CH3:43])[CH3:45])(=[O:38])[CH:36]=[CH2:37].[C:29]([NH2:33])(=[O:32])[CH:30]=[CH2:31]

Komponenten

8

Edukt 6

HCID 1118Sulfuric AcidHCID 6144Edetate SodiumHCID 6579AcrylamideHCID 162071Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1)HCID 3476271Methyl 3-(1,3-benzodioxol-5-ylmethylsulfamoyl)thiophene-2-carboxylateHCID 23668195Sodium Bromate

Produkt 1

HCID 155211Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

An organic solution is prepared by combining a low odor paraffin oil (208.4 g), polyoxyethylene sorbitan monooleate (9.0 g) and polyoxyethylene sorbitan trioleate (32.6 g) in a reactor with stirring. To this solution is added an aqueous solution, adjusted to pH=3.5 with sulfuric acid, containing acrylamide (24.0 g), acryloxyethyltrimethyl ammonium chloride (80.2 g), sodium bromate (0.01 g), ethylenediaminetetraacetic acid tetra sodium salt (0.21 g), and water (145.58 g).

Aufarbeitung

  1. customAn organic solution is prepared
  2. additionTo this solution is added an aqueous solution

Quellen und Nachweise

ORD-Eintrag
ord-7498b1744f9b4529a5cdb48a5cb9a9d4
Quelldatensatz
uspto-grants-1999_03
Patentnummer
US05883181

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