Benzoic Acid → HCID 178443205, Verbindung

HRID 1517221

Reaktionsgleichung

Reaktionsgleichung von HRID 1517221
[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N+:14]([CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH3:16])[CH3:15].[C:24]([OH:32])(=[O:31])[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1.[OH2:33]>CC(C)=O>[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N+:14]([CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH3:16])[CH3:15].[C:24]([O-:32])(=[O:31])[C:25]1[C:30](=[CH:29][CH:28]=[CH:27][CH:26]=1)[OH:33]

Komponenten

5

Edukt 3

HCID 243Benzoic AcidHCID 962WaterHCID 2330Benzalkonium

Produkt 1

HCID 178443205HCID 178443205, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 180AcetoneLösungsmittel

Versuchsvorschrift

Benzalkonium saccharinate (0.01 mol) and benzoic acid (0.01 mol) were dissolved in 25 mL of hot acetone. The mixture was stirred at room temperature for 5 h. Distilled water was added. The organic phase was separated and washed with distilled water. Organic phase was evaporated and the product, benzalkonium salicylate, was dried under vacuum. 1H and 13C NMR (DMSO) were obtained.

Aufarbeitung

  1. customThe organic phase was separated
  2. washwashed with distilled water
  3. customOrganic phase was evaporated
  4. dry with materialthe product, benzalkonium salicylate, was dried under vacuum
  5. custom1H and 13C NMR (DMSO) were obtained

Quellen und Nachweise

ORD-Eintrag
ord-e03584b9ee594ae3a3e87f092de87697
Quelldatensatz
uspto-grants-2012_07
Patentnummer
US08232265B2

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