Chloride → N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

HRID 1578421Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1578421
[CH2:1]([Cl:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH3:23])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Cl-]>>[Cl-:4].[CH2:1]([N+:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:5])[CH3:23])[CH:2]=[CH2:3]

Komponenten

4

Edukt 3

HCID 312ChlorideHCID 7850Allyl chlorideHCID 16221Dimethylhexadecylamine

Produkt 1

HCID 20503036N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

Versuchsvorschrift

Allyl hexadecyl dimethyl ammonium chloride was prepared by reacting allyl chloride and dimethyl hexadecyl amine as set forth in Example 1. 17.8 grams of the chloride in 23.5% aqueous solution were treated with a stoichiometric excess of AgF in aqueous solution until analysis of the filtrate showed only a trace of chloride ion present. Excess silver ion was removed by the careful addition of NaCl, AgCl being removed by filtration.

Aufarbeitung

  1. customExcess silver ion was removed by the careful addition of NaCl, AgCl being
  2. customremoved by filtration

Quellen und Nachweise

ORD-Eintrag
ord-a8f58aa3c9c247dcace3ebd4b203704a
Quelldatensatz
uspto-grants-1976_02
Patentnummer
US03936492

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