Sodium Fluoride → Phenyl Fluoroformate
Reaktionsgleichung
[C:1]1([O:7][C:8](Cl)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[F-:11].[Na+].C1OCCOCCOCCOCCOC1>C(#N)C>[C:1]1([O:7][C:8]([F:11])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 40 °C
Versuchsvorschrift
To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5 (“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).
Aufarbeitung
- customReaction completion
Quellen und Nachweise
- ORD-Eintrag
- ord-8b9ce016ec564ff58f9729c1d8df04f0
- Quelldatensatz
- uspto-grants-2001_09
- Patentnummer
- US06284911B1
Notizen zur Reaktion
Wird geladen…