Acetophenone → N-(1-phenylethyl)formamide
Reaktionsgleichung
[CH:1]([O-:3])=O.[NH4+:4].[C:5]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=O)[CH3:6]>C(O)=O>[CH:1]([NH:4][CH:5]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH3:6])=[O:3]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
In the same manner as in Example 1 except that a mixture of formic acid, ammonium formate and acetophenone was heated with stirring at 160° C. for 6 hours in place of the concurrent addition of acetophenone and formic acid to ammonium formate for 3 hours and keeping the mass after the addition stirred for 3 hours, the reaction and post treatment were carried out to obtain 112 g of crude N-formyl-1-phenylethylamine; the purity: 82.7%
Aufarbeitung
- temperaturewas heated
- additionafter the addition
- customthe reaction and post treatment
Quellen und Nachweise
- ORD-Eintrag
- ord-3901798a5f584afdad68e09ff1caa5c0
- Quelldatensatz
- uspto-grants-1998_04
- Patentnummer
- US05739401
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