1-Octanol → Dicaprylyl Ether

HRID 1719986

Reaktionsgleichung

Reaktionsgleichung von HRID 1719986
[CH2:1]([OH:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S([CH:14]([CH2:18][C:19](O)=O)[C:15](O)=O)(O)(=O)=O>O>[CH2:1]([O:9][CH2:15][CH2:14][CH2:18][CH2:19][CH2:1][CH2:2][CH2:3][CH3:4])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Komponenten

4

Edukt 2

HCID 9571-OctanolHCID 21220Sulfosuccinic acid monosodium salt

Produkt 1

HCID 12399Dicaprylyl Ether

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.

Aufarbeitung

  1. customformed
  2. distillationwas distilled off
  3. addition10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization
  4. washafter which the crude product was washed until neutral and
  5. distillationthen distilled

Quellen und Nachweise

ORD-Eintrag
ord-e296b566e6b848bf9c01de3be92734cb
Quelldatensatz
uspto-grants-1996_04
Patentnummer
US05503760

Verknüpfte Notizen

Wird geladen…