Ethylamine → 4-Ethylamino-3-nitrobenzamide

HRID 1729581

Reaktionsgleichung

Reaktionsgleichung von HRID 1729581
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1Cl)[C:7]([NH2:9])=[O:8])([O-:3])=[O:2].[CH2:14]([NH2:16])[CH3:15]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[NH:16][CH2:14][CH3:15])[C:7]([NH2:9])=[O:8])([O-:3])=[O:2]

Komponenten

3

Edukt 2

HCID 6341EthylamineHCID 279424-Chloro-3-nitrobenzamide

Produkt 1

HCID 37089224-Ethylamino-3-nitrobenzamide

Versuchsvorschrift

II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).

Aufarbeitung

  1. temperatureThe mixture was cooled
  2. customthe precipitate was collected
  3. customcrystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product)

Quellen und Nachweise

ORD-Eintrag
ord-bb3097a7e15a44488e01fcb467723d81
Quelldatensatz
uspto-grants-1976_11
Patentnummer
US03989522

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