Levulinic Acid → Cesium levulinate

HRID 1757030Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1757030
[C:1]([OH:8])(=[O:7])[CH2:2][CH2:3][C:4]([CH3:6])=[O:5].[OH-].[Cs+:10]>O>[C:1]([O-:8])(=[O:7])[CH2:2][CH2:3][C:4]([CH3:6])=[O:5].[Cs+:10]

Komponenten

4

Reaktionsbedingungen

Temperatur
65 °C

Versuchsvorschrift

46.9 gr. of 99% pure levulinic acid is sluurried in 100 cc. distilled water. 97.3 g. of a 4.22 molar, pure cesium hydroxide solution is added and the temperature is raised to 65° C. to obtain complete solution. The solution is filtered through No. 40 filter paper to remove dust, etc. The solution is then evaporated on a hot plate to 200 g., which gives a 2 molar concentration, and it is then bottled. These materials are readily compounded into highly stable solutions which can be readily coated onto a variety of substrates. The preparation of a sensor solution of cesium benzoylpropionate, which triggers optically at 35% RH at 20° C. (when applied as a film); typifies the preparation of sensors useful for lower RH sensing.

Aufarbeitung

  1. customto obtain complete solution
  2. filtrationThe solution is filtered through No
  3. filtration40 filter paper
  4. customto remove dust, etc. The solution
  5. customis then evaporated on a hot plate to 200 g
  6. custom, which gives
  7. concentrationa 2 molar concentration, and it
  8. customThe preparation of a sensor solution of cesium benzoylpropionate, which
  9. customtriggers optically at 35% RH at 20° C.
  10. customthe preparation of sensors useful for lower RH sensing

Quellen und Nachweise

ORD-Eintrag
ord-d13e1c25456248979d2c44affae8a1f5
Quelldatensatz
uspto-grants-1995_08
Patentnummer
US05443753

Notizen zur Reaktion

Wird geladen…