1-Methylimidazole → HCID 131719089, Verbindung
Reaktionsgleichung
C(=O)([O-])[O-].[Co+2:5].[CH:6](=[O:14])[C:7]1[C:8](=[CH:10][CH:11]=[CH:12][CH:13]=1)[OH:9].[CH3:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1>>[CH3:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1.[CH3:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1.[Co+2:5].[CH:6](=[O:14])[C:7]1[C:8](=[CH:10][CH:11]=[CH:12][CH:13]=1)[OH:9].[CH:6](=[O:14])[C:7]1[C:8](=[CH:10][CH:11]=[CH:12][CH:13]=1)[OH:9]Komponenten
4
Versuchsvorschrift
1 mole of cobalt (II) carbonate was thoroughly mixed with 2 moles of salicylaldehyde with an excess of 1-methyl imidazole at moderate temperatures using the procedure of Example 1 to obtain a 97% yield of bis-(salicylaldehyde)-cobalt (II) di(1-methylimidazole)
Quellen und Nachweise
- ORD-Eintrag
- ord-ae1f7ea938cc4857adccff19448cce16