Ethyl octanoate → Octanoic hydrazide

HRID 1863201

Reaktionsgleichung

Reaktionsgleichung von HRID 1863201
[C:1]([O:10]CC)(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].O.[NH2:14][NH2:15]>C(O)C>[C:1]([NH:14][NH2:15])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Komponenten

4

Edukt 2

HCID 7799Ethyl octanoateHCID 24654Hydrazine hydrate (1:1)

Produkt 1

HCID 80556Octanoic hydrazide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Production of the spacer-gel derivative: Ethyl caprylate was converted into the corresponding hydrazide by hydrazinolysis, by initially admixing 10 ml. of this ethyl ester with 10 ml. of 98% hydrazine hydrate. Ethanol (22 ml.) was added as solvent, until the reaction mixture cleared, following which the solution was left at room temperature for 15 hours. The crystallized out resulting caprylhydrazide was filtered off and washed with ice water and then with aqueous methanol (1:1) of room temperature.

Aufarbeitung

  1. customThe crystallized

Quellen und Nachweise

ORD-Eintrag
ord-30a09d1cae444aae8f82551b262200ee
Quelldatensatz
uspto-grants-1979_09
Patentnummer
US04168300

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