Morpholine → Chloromethyl 4-morpholinecarboxylate

Reaktionsgleichung

[Cl:1][CH2:2][O:3][C:4](Cl)=[O:5].[NH:7]1[CH2:12][CH2:11][O:10][CH2:9][CH2:8]1>>[Cl:1][CH2:2][O:3][C:4]([N:7]1[CH2:12][CH2:11][O:10][CH2:9][CH2:8]1)=[O:5]

Komponenten

Edukt 2

HCID 8083Morpholine

HCID 62754Chloromethyl chloroformate

Produkt 1

HCID 23371992Chloromethyl 4-morpholinecarboxylate

Versuchsvorschrift

Using chloroformic acid chloromethyl ester and morpholine as the raw materials, the same operation as the Example 101(1) gave the title compound as a crude product, and the crude product was used for the next reaction without further purification.

Quellen und Nachweise

ORD-Eintrag: ord-924caf96a43f48ab8682aec18268a6f8
Quelldatensatz: uspto-grants-2009_12
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07626042B2

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