Water → Aluminum Chloride Hydrate Thiourea

HRID 1902817

Reaktionsgleichung

Reaktionsgleichung von HRID 1902817
[OH2:1].O.O.O.O.O.[Cl-:7].[Al+3:8].[Cl-].[Cl-].[NH2:11][C:12]([NH2:14])=[S:13].O>>[OH2:1].[Cl-:7].[Al+3:8].[Cl-:7].[Cl-:7].[NH2:11][C:12]([NH2:14])=[S:13]

Komponenten

4

Edukt 3

HCID 962WaterHCID 2723790ThioureaHCID 9794789AlCl3.6H2O

Produkt 1

HCID 86738713Aluminum Chloride Hydrate Thiourea

Reaktionsbedingungen

Temperatur
72 °C

Versuchsvorschrift

In a 5 liter flask is placed 482.8 g. (2.0 mole) aluminum chloride hexahydrate and 1826.8 g. (24.0 moles) thiourea and shaken to mix. To this is added 2284 g. (127 moles) water and heated with stirring to 72° C. to obtain a clear, colorless solution. White crystals form upon cooling leaving a clear solution of pH 1.7 and a final weight of 4592 g.

Aufarbeitung

  1. customIn a 5 liter flask is placed
  2. additionto mix
  3. additionTo this is added 2284 g
  4. customto obtain a clear, colorless solution
  5. customWhite crystals form
  6. temperatureupon cooling
  7. customleaving a clear solution of pH 1.7

Quellen und Nachweise

ORD-Eintrag
ord-92eb2987676b43159ef2fe9e790f12cd
Quelldatensatz
uspto-grants-1982_12
Patentnummer
US04366096

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