Acetic Acid → HCID 67239262, Verbindung

HRID 1963680Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1963680
C(O[C:9]1[CH:14]=[C:13]([S:15]([C:18]2[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][CH:19]=2)(=[O:17])=[O:16])[C:12]([F:26])=[CH:11][C:10]=1[C:27]1[CH:32]=[CH:31][CH:30]=[C:29]([F:33])[CH:28]=1)C1C=CC=CC=1.[H][H].C(O)(=[O:38])C>[Pd]>[F:26][C:12]1[CH:11]=[C:10]([C:27]2[C:32]([OH:38])=[CH:31][CH:30]=[C:29]([F:33])[CH:28]=2)[CH:9]=[CH:14][C:13]=1[S:15]([C:18]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][CH:19]=1)(=[O:16])=[O:17]

Komponenten

5

Edukt 3

HCID 176Acetic AcidHCID 68089499HCID 68089499, VerbindungHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 67239262HCID 67239262, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 23938PalladiumKatalysator

Versuchsvorschrift

A suspension of the product of step (ii) (838 mg) in acetic acid (30 ml) and 10% Pd/C (200 mg) was stirred under 2 bar pressure of hydrogen for 30 min. The catalyst was removed by filtration and the filtrate was evaporated to give the subtitle compound, yield 630 mg.

Aufarbeitung

  1. customThe catalyst was removed by filtration
  2. customthe filtrate was evaporated

Quellen und Nachweise

ORD-Eintrag
ord-9d80e81b84a043689c79567b3e3b7abd
Quelldatensatz
uspto-grants-2013_04
Patentnummer
US08415394B2

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