Ethylenediaminetetraacetic Acid → Acrylamide Dimethylaminoethyl Acrylate Methyl chloride

HRID 1978796

Reaktionsgleichung

Reaktionsgleichung von HRID 1978796
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH3:6][Cl:7].[C:8]([O:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16])(=[O:11])[CH:9]=[CH2:10].C(N(CC(O)=O)CC(O)=O)CN(CC(O)=O)CC(O)=O.C1C(C(N)=O)=CN(C2OC(COP(OP(OCC3OC(N4C5N=CN=C(N)C=5N=C4)C(OP([O-])([O-])=O)C3O)([O-])=O)([O-])=O)C(O)C2O)C=C1.[Na+].[Na+].[Na+].[Na+].S([O-])([O-])(=O)=O.[NH4+].[NH4+].S([O-])([O-])(=O)=O.[Na+].[Na+]>[Cl-].C([N+](CC=C)(C)C)C=C.O>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH3:6][Cl:7].[C:8]([O:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16])(=[O:11])[CH:9]=[CH2:10]

Komponenten

9

Edukt 6

HCID 6049Ethylenediaminetetraacetic AcidHCID 6579AcrylamideHCID 24436Sodium SulfateHCID 6097028Ammonium SulfateHCID 12598259[2-adenin-9-yl-5-[[[[5-(3-carbamoyl-4H-pyridin-1-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methoxy-oxido-phosphoryl]oxy-oxido-phosphoryl]oxymethyl]-4-hydroxy-tetrahydrofuran-3-yl] phosphateHCID 22395581Dimethylaminoethyl acrylate methylchloride2×

Produkt 1

HCID 86644221Acrylamide Dimethylaminoethyl Acrylate Methyl chloride

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 33286Diallyldimethylammonium chlorideKatalysator3×HCID 962WaterLösungsmittel

Versuchsvorschrift

A 20.2% polymer solids, 60/30/10 mole percent acrylamide/dimethylaminoethyl acrylate methyl chloride quaternary salt/diallyldimethyl ammonium chloride dispersion polymer was synthesized in a method similar to that described in Example 1. To the reactor setup described above was added 22.4 g of acrylamide (48.9% aqueous solution), 18.6 g of dimethylaminoethyl acrylate methyl chloride quaternary salt (80% aqueous solution), 44.3 g of diallyldimethyl ammonium chloride (62.4% aqueous solution), 60.0 g of a homopolymer of dimethylaminoethyl acrylate methyl chloride quaternary (15% aqueous solution, available from Nalco Chemical Company), 45 g of a homopolymer of diallyldimethyl ammonium chloride (15% aqueous solution), 12.0 g of polyethylene glycol (mw. 400), 0.1 g of ethylenediaminetetraacetic acid, tetra sodium salt, 190.0 g of ammonium sulfate, 50.0 g sodium sulfate, and 300.0 g of deionized water.

Quellen und Nachweise

ORD-Eintrag
ord-8721777bc8bd4828b48484c01d92b5f1
Quelldatensatz
uspto-grants-2001_05
Patentnummer
US06238486B1

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