Toluene → Oleylamine styrene oxide

HRID 1982144

Reaktionsgleichung

Reaktionsgleichung von HRID 1982144
[B].[CH2:2]([NH2:20])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]/[CH:10]=[CH:11]\[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH2:21]1[O:29][CH:22]1[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1.C1(C)C=CC=CC=1>O>[CH2:2]([NH2:20])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]/[CH:10]=[CH:11]\[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH2:21]1[O:29][CH:22]1[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Komponenten

6

Edukt 4

HCID 1140TolueneHCID 7276Styrene OxideHCID 5356789OleylamineHCID 5462311Boron

Produkt 1

HCID 86740542Oleylamine styrene oxide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A sulfurized, boron-containing, heterocyclic compound is prepared by mixing 12 grams of oleylamine, 9.6 grams of styrene oxide and 200 ml of toluene for 30 minutes at room temperature (25° C.) in a single-necked one-liter round-bottomed flask. The flask is placed in a heating mantle and equipped with a water-cooled condenser. The mixture is heated under reflux for three hours producing an oleylamine/styrene oxide adduct.

Aufarbeitung

  1. temperaturecooled condenser
  2. temperatureThe mixture is heated
  3. temperatureunder reflux for three hours

Quellen und Nachweise

ORD-Eintrag
ord-80e74dfb277c499ea67e61ae01fcddfc
Quelldatensatz
uspto-grants-1986_06
Patentnummer
US04595514

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