1,2-Dichloroethane → HCID 131716892, Verbindung

HRID 2051102Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2051102
[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]>O>[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]

Komponenten

4

Edukt 2

HCID 111,2-Dichloroethane4×HCID 117779L-Lysine, methyl ester3×

Produkt 1

HCID 131716892HCID 131716892, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A 0.4%(w/w) solution of HA in water was prepared. The pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid. To each 100 ml of this solution was added 0.76 g of EDC with stirring until the EDC had completely dissolved. To each 100 ml of the HA/EDC solution was added 0.20 g of lysine methyl ester (LME) with stirring until the LME had completely dissolved. The addition of HA, EDC, and LME was conducted at room temperature; once the final HA/EDC/LME solution had been formed, it was stored at 4° C. until needed.

Aufarbeitung

  1. additionThe pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid
  2. dissolutionhad completely dissolved
  3. dissolutionhad completely dissolved
  4. customwas conducted at room temperature

Quellen und Nachweise

ORD-Eintrag
ord-d32febacb24e4c3085b21e4c9751b5c0
Quelldatensatz
uspto-grants-1991_05
Patentnummer
US05017229

Notizen zur Reaktion

Wird geladen…