Allyl chloride → N-(2,2-Dimethoxyethyl)prop-2-en-1-amine

Reaktionsgleichung

[CH3:1][O:2][CH:3]([O:6][CH3:7])[CH2:4][NH2:5].[CH2:8](Cl)[CH:9]=[CH2:10]>>[CH2:10]([NH:5][CH2:4][CH:3]([O:6][CH3:7])[O:2][CH3:1])[CH:9]=[CH2:8]

Komponenten

Edukt 2

HCID 7850Allyl chloride

HCID 89728Aminoacetaldehyde dimethyl acetal

Produkt 1

HCID 13334742N-(2,2-Dimethoxyethyl)prop-2-en-1-amine

Versuchsvorschrift

Aminoacetaldehyde dimethyl acetal was reacted with allyl chloride to give N-allyl-N-dimethoxyethyl amine, which was then acetylated with acetyl chloride to give N-allyl-N-dimethoxyethyl acetamide, according to the following reactions: ##STR3##

Quellen und Nachweise

ORD-Eintrag: ord-bbc00a841aee40ea8fdcf578ba238265
Quelldatensatz: uspto-grants-1993_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05187006

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