Di-tert-butyl dicarbonate → HCID 68477709, Verbindung

HRID 2089573Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2089573
[CH3:1][C:2]1[CH:3]=[C:4]2[C:8](=[C:9]([N+:11]([O-:13])=[O:12])[CH:10]=1)[NH:7][C:6]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[CH:5]2.[O:20](C(OC(C)(C)C)=O)[C:21]([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=O>CN(C1C=CN=CC=1)C>[C:21]([N:7]1[C:8]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:10][C:9]=2[N+:11]([O-:13])=[O:12])[CH:5]=[C:6]1[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:20]

Komponenten

4

Edukt 2

HCID 90495Di-tert-butyl dicarbonateHCID 68477399HCID 68477399, Verbindung

Produkt 1

HCID 68477709HCID 68477709, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 142844-(Dimethylamino)pyridineKatalysator

Versuchsvorschrift

5-Methyl-7-nitro-2-phenyl-1H-indole prepared in Preparation 24, (BOC)2O and DMAP were reacted according to the same procedure as Preparation 23 to give the title compound.

Aufarbeitung

  1. customwere reacted
  2. customaccording to the same procedure as Preparation 23

Quellen und Nachweise

ORD-Eintrag
ord-b540a8308a694a92a8ccfecf40504f4c
Quelldatensatz
uspto-grants-2013_05
Patentnummer
US08436038B2

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