Acetone → Pyrogallol

HRID 2231171

Reaktionsgleichung

Reaktionsgleichung von HRID 2231171
[Al].[CH3:2][C:3]([CH3:5])=[O:4].C(OCCOC)(=[O:8])C.[CH2:14]([C:16](C)=[O:17])[CH3:15]>>[C:3]1([CH:5]=[CH:15][CH:14]=[C:16]([OH:17])[C:2]=1[OH:8])[OH:4]

Komponenten

5

Reaktionsbedingungen

Temperatur
70 °C

Versuchsvorschrift

Both surfaces of a 0.24 mm thick aluminum plate were sand-grained using a nylon brush and an aqueous dispersion of 400 mesh pumice stone and thoroughly washed with water. This aluminum plate was dipped in a 5% aqueous solution of sodium triphosphate maintained at 70° C. for 3 minutes, washed with water, and dried. A photo-sensitive solution as described in British Pat. No. 1,113,759 was prepared by dissolving 1 part by weight of a naphthoquinone-1,2-diazido-5-sulfonic acid ester of polyhydroxyphenyl obtained by polycondensation of acetone and pyrogallol and 2 parts by weight of a novolak type phenol-formaldehyde resin in a mixed solvent of 20 parts by weight of 2-methoxyethyl acetate and 20 parts by weight of methyl ethyl ketone. This photo-sensitive solution was coated on one surface of the above-prepared plate and then on the other surface to produce a pre-sensitized printing plate which has photo-sensitive layers on both surfaces of the plate. The thus-produced printing plate was cut in three 1,003 mm×800 mm pieces to produce Samples A, B and C.

Aufarbeitung

  1. washan aqueous dispersion of 400 mesh pumice stone and thoroughly washed with water
  2. washwashed with water
  3. customdried
  4. custom1,113,759 was prepared

Quellen und Nachweise

ORD-Eintrag
ord-ca2206a8b45444a98381909e690b2598
Quelldatensatz
uspto-grants-1988_11
Patentnummer
US04781941

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