Acetic Anhydride → Magnesium Acetate
Reaktionsgleichung
O.O.O.O.[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11].C(OC(=O)C)(=O)C>>[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11]Komponenten
3
Versuchsvorschrift
Into a 300 ml. flask equipped as in EXAMPLE I and maintained under a nitrogen atmosphere were added 21.5 grams magnesium acetate tetrahydrate and 80 ml. acetic anhydride and the mixture was heated at the reflux temperature for 1 hour. After cooling, a clear liquid was drawn off and the remaining solid was dried at 35° C. under a vacuum of 0.3 mm mercury for several hours to obtain anhydrous magnesium acetate.
Aufarbeitung
- customflask equipped as in EXAMPLE I
- temperaturemaintained under a nitrogen atmosphere
- temperatureAfter cooling
- dry with materialthe remaining solid was dried at 35° C. under a vacuum of 0.3 mm mercury for several hours
Quellen und Nachweise
- ORD-Eintrag
- ord-9897bfdbe8794d8db29d28f904ee8c59
- Quelldatensatz
- uspto-grants-1980_11
- Patentnummer
- US04233253
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