[CH2:1](O)[CH3:2].CC([O:9][C:10](C)=[O:11])COC.CCO[Si]([O:23][CH2:24][CH3:25])(OCC)OCC.[N+]([O-])(O)=[O:27].[CH2:30]([OH:34])[CH2:31][CH2:32][CH3:33]>O>[CH:1]1[C:31]([C:30]([OH:27])=[O:34])=[CH:32][C:33]2[C:10]([O:11][C:24](=[O:23])[C:25]=2[CH:2]=1)=[O:9]
To the solvents of 60 g ethanol and 30 g PGMEA, 33.33 g TEOS, 5.71 g VTEOS and 2.40 g PTEOS monomers were individually added. While stirring a mixture of 1.13 g 0.1N nitric acid and 18.92 g water was poured, the reaction mixture was heated to reflux at 81° C. for 4 hours before cooling down. 8.84 g butanol was added to the reaction mixture and stirred at room temperature overnight. The resulting polymer was measured to have a molecular weight of Mn=1121 amu, Mw=1723 amu analyzed using the same GPC system as mentioned above.
Wird geladen…
