4-Nitrobenzoic Acid → 4-Nitro-N-(3-(trifluoromethyl)phenyl)benzamide
Reaktionsgleichung
[F:1][C:2]([F:11])([F:10])[C:3]1[CH:4]=[C:5]([CH:7]=[CH:8][CH:9]=1)[NH2:6].[N+:12]([C:15]1[CH:23]=[CH:22][C:18]([C:19](O)=[O:20])=[CH:17][CH:16]=1)([O-:14])=[O:13]>>[N+:12]([C:15]1[CH:16]=[CH:17][C:18]([C:19]([NH:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:3]([C:2]([F:10])([F:11])[F:1])[CH:4]=2)=[O:20])=[CH:22][CH:23]=1)([O-:14])=[O:13]Komponenten
3
Versuchsvorschrift
Using 3-trifluoromethylaniline (1.77 g, 11.0 mmol) and 4-nitrobenzoic acid (1.67 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 2.48 g (80.0%) of the title compound in the form of colorless powder.
Quellen und Nachweise
- ORD-Eintrag
- ord-5184ffb1f92a40a8a3af5aec36316d41
- Quelldatensatz
- uspto-grants-1998_03
- Patentnummer
- US05728835
Notizen zur Reaktion
Wird geladen…