4-Iodoaniline → N-(4-iodophenyl)-N-methylethanesulphonamide

HRID 256607

Reaktionsgleichung

Reaktionsgleichung von HRID 256607
[I:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.I[C:10]1C=CC(NS(C)(=O)=O)=CC=1.[CH2:21]([S:23](Cl)(=[O:25])=[O:24])[CH3:22]>>[I:1][C:2]1[CH:8]=[CH:7][C:5]([N:6]([CH3:10])[S:23]([CH2:21][CH3:22])(=[O:25])=[O:24])=[CH:4][CH:3]=1

Komponenten

4

Edukt 3

HCID 108934-IodoanilineHCID 11667Ethanesulfonyl chlorideHCID 836147N-(4-iodophenyl)methanesulfonamide

Produkt 1

HCID 19785600N-(4-iodophenyl)-N-methylethanesulphonamide

Versuchsvorschrift

The product so obtained was used in place of 4-iodoaniline in the procedure described in Example 3 for the preparation of N-(4-iodophenyl) methanesulphonamide and ethanesulphonyl chloride was used in place of methanesulphonyl chloride. Thus was obtained N-(4-iodophenyl)-N-methylethanesulphonamide as an oil. NMR Spectrum 1.45 (3H, t), 3.00 (2H, q), 3.35 (3H, s), 7.15 (2H, m), 7.70 (2H, m).

Aufarbeitung

  1. customThe product so obtained

Quellen und Nachweise

ORD-Eintrag
ord-5611fef512954a2ea8368584f719a99e
Quelldatensatz
uspto-grants-1993_11
Patentnummer
US05258399

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